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4种提取印楝素方法的比较     被引量:10

Comparing Four Azadirachtin Extraction Methods

文献类型:期刊文献

中文题名:4种提取印楝素方法的比较

英文题名:Comparing Four Azadirachtin Extraction Methods

作者:段琼芬[1] 王有琼[1] 孙龙[1] 李晓升[1]

第一作者:段琼芬

机构:[1]中国林业科学研究院资源昆虫研究所

年份:2005

卷号:44

期号:10

起止页码:455-456

中文期刊名:农药

外文期刊名:Pesticides

收录:CSTPCD;;北大核心:【北大核心2004】;

基金:国家林业局"948"资助项目(2002-58)

语种:中文

中文关键词:印楝素;提取方法;比较试验

外文关键词:azadirachtin, extraction method, comparison experiment

分类号:TQ450.7

摘要:做了微波法、超声波法、快速萃取法和常规浸提法试验,考察粗提物及印楝素的提取率。结果粗提物的提取率依次为5.86%、6.36%、6.86%、3.80%,用高压液相法定量测定前3种印楝素的质量分数,计算提取率依次为0.54%、0.55%、0.48%。结论:快速萃取法是一种提取率与微波法相当的简单易行的方法。
Microwave, ultrasonic, rapid extraction, and conventional extraction methods were conducted to investigate the extraction yields of crude extract and azadirachtin; the yields of crude extract were 5.86, 6.36, 6.86, and 3.80, respectively. Using HPLC to quantitatively determine the mass fractions of the first three azadirachtin, extraction yields were 0.54, 0.55, and 0.48, respectively. Thus, the rapid extraction method is simple and convenient to conduct and provided extraction yields eoual to microwave extractionAbstract: Microwave, ultrasonic, rapid extraction, and conventional extraction methods were conducted to investigate the extraction yields of crude extract and azadirachtin; the yields of crude extract were 5.86, 6.36, 6.86, and 3.80, respectively. Using HPLC to quantitatively determine the mass fractions of the first three azadirachtin, extraction yields were 0.54, 0.55, and 0.48, respectively. Thus, the rapid extraction method is simple and convenient to conduct and provided extraction yields equal to microwave extraction.

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